【摘要】：以1,2:5,6-氧-二異亞丙基-α-D-呋喃葡萄糖為原料,依次通過芐基保護(hù)、脫保護(hù)、甲磺�；�、酯交換、環(huán)氧化、水解重排并乙酰化得到標(biāo)題化合物,總產(chǎn)率68.2%。該方法操作簡便,適宜工業(yè)化。
[Abstract]:The title compound was obtained by benzyl protection, deprotection, formylation, transesterification, epoxidation, hydrolysis and rearrangement and acetylation with 1: 2: 5: 6- oxy-diisopropyl- 偽 -Dfuran glucose as raw material. The total yield was 68.2%. The method is simple and suitable for industrialization.
【作者單位】： 貴陽醫(yī)學(xué)院藥學(xué)院;
【基金】：貴州省國際科技合作計(jì)劃項(xiàng)目[黔科合外G字(2013-7025)] 貴州省高等學(xué)校創(chuàng)新能力提升計(jì)劃[黔教合協(xié)同創(chuàng)新字(2013)04] 國家重大科學(xué)儀器設(shè)備開發(fā)專項(xiàng)(2011YQ12003506)
【分類號】：R914.5
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本文編號：2162522